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Lab test

Cortisol, Free and Total, LC/MS Test

This test measures both free and total cortisol concentrations in a blood serum sample. Quest describes free cortisol measurement as used in evaluating Cushing's syndrome, a condition in which free cortisol is elevated.

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About this test

The test analyzes a serum sample, collected in a red-top tube without gel, using equilibrium dialysis combined with chromatography/mass spectrometry (LC/MS). This method reports both the total cortisol concentration and the free, unbound portion.

Quest describes elevated free cortisol concentrations as associated with Cushing's syndrome, and notes that free cortisol measurement is used in evaluating that condition. Reporting free cortisol alongside the total gives a clinician a more complete read than the total value alone.

Test details

CollectionQuest patient service center

Quest resources

Additional details

What this test looks at

The test reports two values from the same sample: total cortisol and free cortisol, both measured by equilibrium dialysis combined with chromatography/mass spectrometry on a 2 mL serum sample. The LC/MS methodology is a chromatography and mass spectrometry technique that separates and identifies cortisol precisely within the sample.

This test isn't part of the Celio Health store at the moment, so it can't be ordered or requested here. The test menu lists everything that can.

Laboratory results should always be interpreted by a licensed clinician who knows your health history. This page is information about a test, not medical advice.

Frequently asked questions

What does this test measure?

It measures both total and free cortisol concentrations in a serum sample, using equilibrium dialysis combined with chromatography/mass spectrometry.

How is the sample collected?

The test uses a 2 mL serum sample, collected in a red-top tube without gel.

Do I need to prepare for this test?

No preparation instructions are listed for this test, though people follow any instructions their ordering clinician provides.

Why measure free cortisol separately from total cortisol?

Quest describes free cortisol measurement as used in evaluating Cushing's syndrome, a condition in which free cortisol concentrations are elevated, distinct from the total cortisol value.

Last updated 2026-09-18 · How we write about lab testing

Educational content

This page is for general educational purposes only. It is not medical advice, and it is not a substitute for consultation with a qualified healthcare professional. Laboratory results should always be interpreted by a licensed clinician who knows your health history. If you have questions about your health or your results, talk with your doctor. If you think you may be experiencing a medical emergency, call 911.